Note from June 29, 2020
Although we do not yet know how long the social distancing related to the Covid-19 pandemic will last, and regardless of the changes that had to be made in the evaluation of the June 2020 session in relation to what is provided for in this learning unit description, new learnig unit evaluation methods may still be adopted by the teachers; details of these methods have been - or will be - communicated to the students by the teachers, as soon as possible.
Although we do not yet know how long the social distancing related to the Covid-19 pandemic will last, and regardless of the changes that had to be made in the evaluation of the June 2020 session in relation to what is provided for in this learning unit description, new learnig unit evaluation methods may still be adopted by the teachers; details of these methods have been - or will be - communicated to the students by the teachers, as soon as possible.
7 credits
45.0 h + 30.0 h
Q2
Teacher(s)
Cybulska Iwona; Herent Marie-France; Robiette Raphaël (coordinator);
Language
French
Prerequisites
LBIR1318
Main themes
General description of 4 main spectroscopic techniques used in organic analysis: mass spectrometry, nuclear magnetic resonance (proton and carbon), infrared and UV-visible. For each of them are described the basic principles, analytical information which can be used, examples of applications in organic analysis, and the equipment. Seminars and practical classes allow the student to develop a strategy for the identification of organic compounds.
Aims
At the end of this learning unit, the student is able to : | |
| 1 |
The course contributes to the following learning outcomes : 1.1, 1.3, 1.4, 1.5 + 3.4, 3.6, 3.7, 3.8 + 6.3 (BIRC21) At the end of this course, the student will be able to : - analyse mass, UV, NMR and IR spectra of organic compounds belonging to the main chemical families, - develop new protocols for qualitative and quantitative analyses of organic compounds, taking into account the complexity of the matrix (optimal association of extraction procedures, chromatographic analyses and detection techniques), - orally present his results. |
The contribution of this Teaching Unit to the development and command of the skills and learning outcomes of the programme(s) can be accessed at the end of this sheet, in the section entitled “Programmes/courses offering this Teaching Unit”.
Content
Theoretical course. General description of the main spectroscopies. Mass spectrometry: basic principles, analytical information, applications for saturated and unsaturated hydrocarbons, aromatics, alcohols, carbonyles, carboxylic acids and esters, systems of introduction, ionization modes, systems of deflection. Nuclear magnetic resonance: basic principles, chemical shift for H and C, coupling constants, intramolecular mobility, longitudinal and transversal relaxations. Infrared spectrometry: conditions of absorption and modes of vibration, applications for alcanes, alcenes, aromatics, alcohols, carbonyles, halogenic compounds. UV-visible spectroscopy: diagram of Jablonski and types of transitions, applications for alcenes, carbonyles, benzene, solvent effect, equipment.
Teaching methods
Magistral lectures for the theoretical part. Seminars allow to use the new concepts, by analyzing MS (EI, CI, ESI, APCI), NMR, IR and UV-visible spectra. At the laboratory, the student is put in the situation of a researcher, in front of a new problem.
Evaluation methods
Written examination for the theoretical aspects. The experimental know-how and the attitude are evaluated throughout practical classes, as well as by an oral presentation (English) and a report miming the writing of a publication.
Other information
This course can be given in english.
Online resources
Moodle
Bibliography
Le cours ne fait appel à aucun support particulier qui serait payant et jugé obligatoire
Teaching materials
- slides and exercices (moodle)
Faculty or entity
AGRO
Programmes / formations proposant cette unité d'enseignement (UE)
Title of the programme
Sigle
Credits
Prerequisites
Aims
Master [120] in Chemistry and Bioindustries
